How to use an alkaline beam test for CBD?
Tired of “guessing” when my reactions are done.
4 Likes
equipment?!?
5% KOH in ethanol!!!
concerned about your “reactions” if you need a kit to achieve this…
3 Likes
Should have rephrased it…
I just used equipment as a catch all because of all the new cool shit people keep finding. Wasn’t sure what was available
please do. it still doesn’t make sense…
amazon sells KOH, my local liquor store sells ever clear.
here is a writeup from ICMAG
7 Likes
So just KOH with ethanol and my reaction solution and watch for the color change?
I’m not one for analytics (starting to get into it now) so I’m new to all this.
1 Like
Ughhh… gotta create an account.
BRB
yes. its so simple even the cops can perform that one.
if that’s news, I’m concerned about the those “reactions”.
1 Like
Never had my shit tested by the cops so wouldn’t know 
I try to avoid that “lab”
Just needed clarification
1 Like
Make a solution of ethanol and potassium hydroxide where the KOH is 5% of the total weight of the solution.
3 Likes
Thank ya!
2 Likes
care of @Photon_noir
Alkaline Beam Test: Colorimetric testing for CBD
Preparation of Solution & Workspace
- Fill plastic graduated cylinder with about 70mL of 95% ethanol.
- Weigh out 4g KOH on wax paper and add it to alcohol.
- Swirl or stir with stainless or glass rod to dissolve all KOH.
- Finish filling graduated cylinder up to 100mL line with ethanol
- Label the clean glass jar “5% KOH in EtOH, CBD Beam Test” or similar, then pour the entire solutioninto the jar and seal the lid. Swirl a bit to mix well.
- On a paper towel next to the jar, write “Beam” or similar and place a new plastic pipette on it.
- On another paper towel next to the reactor, write “RXN” or similar and place a new plastic pipette onit, also.
- Set up several test tubes with lids in a rack next to the KOH solution and Beam pipette.
☆ Sampling & Testing
- Squirt the rxn solution sample into the uncapped test tube in the rack.
- Unseal the jar and remove the lid (or lid ring) to pull a little bit of KOH test soln from it. Only a fewdrops are needed.
- Squeeze one (1) drop test soln into the tube with the rxn sample and swirl the tube for 2 seconds tomix.
- Observe the color after 5 seconds. If color is light or invisible, add 1 to 3 more drops of KOH soln,swirl 2s. Odd color may show up upon resting for too long or excessive stirring, so only read color reactions that occur immediately (i.e. 1st color under 30 seconds).
7. Take notes with time and dispose of sample.
if you’d like to buy that, I’m happy to take donations.
31 Likes
And thank ya for the title change… was about to do it😂
1 Like
kind of a different topic but isnt there a similar quick and simple test you can do to determine if decarb is complete?
Maybe we can add that to this short thread and make the title represent both processes. (i did a search and couldnt find it but swear i have seen it here somewhere)
4 Likes
bromocresol green. It’s in Tricks of the trade - #655 by CdpIchem
And I’ve linked it in multiple other places…
9 Likes
Thanks!! I knew you would know where it was.
6 Likes
Great idea!
2 Likes
I’m betting the TLC plate can be replaced with a filter paper…
2 Likes
Oddly, it does not! Lower right hand corner of a TLC plate are samples of a decarb product and a crude sample. The center is a paper filter and the ones on the right were spotted on plain paper. Interesting, no?
8 Likes
Thank you!
Pity.
Great thing about being wrong is I learned something 
14 Likes