The oils obtained by the disclosed methods have enhanced sensory and oxidative stabilities. The stability of these product compositions can be determined by measuring, for example, the peroxide value of the compositions. Peroxide value (PV) refers to the concentration of peroxide compounds in the oil measured in meq/kg. Peroxide compounds are produced during oxidation of the oil; thus, an increased peroxide value after a period of time, as compared to initial peroxide values at the initial time, indicates that oxidation has occurred. The peroxide value of the product oils can be minimized by reducing the formation of peroxides or by removing/decomposing the peroxides present in the oil. Thus, the oils prepared according to the methods described herein have minimized peroxide values due to the use of the antioxidants as described herein. Any method for measuring the peroxide values of an oil as known in the art can be used in the methods described herein, such as, for example, AOCS Cd 8-53, which is incorporated by reference herein in its entirety.
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The disclosed products can also contain low levels of oxidized fatty acids and/or aldehydes. For example, many oils containing unsaturated fatty acids can oxidize and break down, resulting in the production of volatile aldehydes like hexanal and a non-volatile portion of the oxidized fatty acid, which remains part of the composition. The products disclosed herein can have reduced levels of such oxidized fatty acids and/or aldehydes, as compared to other marine oils.
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Alternative Methods
In one aspect, the disclosed methods can also involve a bleaching step. The bleaching step can occur before the oil is combined with the antioxidant composition or after the oil and antioxidant composition are combined, yet before deodorization. Thus, in one embodiment, the disclose method comprises the step of combining a bleached oil and antioxidant composition as disclosed herein before deodorization. In an alternative embodiment, the disclosed method comprises the step of combining an oil and antioxidant composition as disclosed herein, bleaching the oil, and then deodorization.
In still a further embodiment, the oil can be contacted with a tocopherol, bleached, combined with the antioxidant composition comprising a green tea extract, and deodorized.
Bleaching oil can be performed by contacting the oil with an adsorbent to provide a mixture, heating the mixture to from about 100 to about 210° C(Adjust temps for use with cannabinoids)., and removing the adsorbent from the mixture, to provide the bleached oil. Suitable adsorbent can be silica, clay, carbon, or a mixture thereof.