Base bath. Be careful though.
Alcojet Low Foaming Powdered Detergent | Alconox Inc.
Alcojet low-foaming, nonionic detergent offers residue-free critical cleaning. For use in ultrasonic cleaning, labware washers, power-spray systems & more.
Base bath. Be careful though.
It’s not exactly the same, but when I couldn’t get the stains off my wiper evaporator, I used to soak it in limonene.
acetone works well
Acetone has been tried
this one has come up a couple or ten times…and there are some great solutions (including piranha) offered.
If you haven’t explored them all, I highly () recommend doing so.
Don’t try this one at home…
Aqua regia is one thing, great for inorganic contaminants and quite good for organics. But if you want ultimate cleanliness from organic contaminants, you want what’s called piranha solution – h2s04 and 30% hydrogen peroxide. It fits the name and has fascinating chemistry such as the production of atomic oxygen as active cleaning agent.
that’s the one I was looking for.
I remember it from another thread but could not remember the name for the life of me.
thank you!
No worries at all my friend
Soak it in a base bath (8M NaOH) or acid bath (70% nitric acid) in a fumehood. Leave it overnight. Rinse with several volumes of water. Then try your organic solvents again.
Do you have access to a sonicator? Usually helps with stubborn grime on our parts.
AlcoJet might work too,
Alconox. Alcojet is the low foam version for use in dishwashers.
Alcojet low-foaming, nonionic detergent offers residue-free critical cleaning. For use in ultrasonic cleaning, labware washers, power-spray systems & more.
I use a bunch of quartz or stainless beads to help when I’m scrubbing a nasty residue off.
https://www.amazon.com/QCQIANG-Precision-Assortment-Bicycles-Refrigerators/dp/B09DJY8FL8/
Yeah, I was thinking another alconox product, Keylajet. I’ve used keylajet before but it’s very basic
That sounds like a direct ketamine delivery system
We’ve had luck before with a 50/50 mix of water and solvent (we use ethanol), put a steel wool pad inside the glass with the mixture, plug the holes with anything from your hands to paper towels. Then swirl that around by hand for better control. If you can get the solvent mixture a little warm that will help too. Cleaning with the stir bar might work in this scenario but I highly recommend agitating by hand to ensure the steel wool and solvent mixture is making adequate contact with the stain. Good luck!
this works wonders, don’t leave it soaking for too long though - it works by slightly etching the glass surface.
Right, good to mention that this will weld sintered glass shut and can eat away at important delicate structures in glass. Otherwise base blast it.
Along the lines of aqua regia, this is another “at your own risk” option (that I do not suggest, but is sold by a reputable scientific supply company):
Shop Chemglass Life Sciences Individual Tool, Rotary Scraper, Fits 5,000mL Round Bottom Flasks at Fishersci.com