Thanks so much, really great ingo. This is something im geting into
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Why is THC-P fragile at 70c+? What happens to it?
I am assuming the exact same thing will happen to thc-p as it does to thc when using alcl3
As a result if not al reactants are removed your presides 9 compound will isomerize to 8 and you can t flip it back
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So quenching is the main problem,
So far the route looks like:
Pottasium Sulphate
Naoh 15% in DCM/ as solid
Wash with DI water
Activated carbon Scrub
Filtration
Drying
If I am not mistaking - but I surely am
That s one way to do it yes carbon scrub 2X at least is my advice