YOC Dirty Diamond Tek - THCa isolation from Crude

Been there, done that…full speed is not the right place to start

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You gotta ease her into it. Also may I suggest using plastic jars aor tubes.

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You can, but stainless is my preference.

Should have full speed capabilities on these by end of day…

Using something much like @pdxcanna suggests above (below)

Just got to get the manufacturing off the inserts…

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Oh that’s nice… Send me a few :sweat_smile:

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Hmm Interesting I’ll give it a try

Still not a good idea.
Backing off by 50%

:frowning:

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What is full speed?

I’d like to find a slip roller and spot weld some stainless mesh around the diameter as reinforcement

Stronger baskets seem to be the ideal route at this poinnt

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4000rpm == 3220 rcf

2000rpm == 805 rcf

RPM / RCF conversion Says those numbers are consistent with ~180mm radius, which is right about where my tape measure puts it.

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You know you can change the fuge to read out rcf instead of rpms :slight_smile:

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Yes.

I used web to double check Carol’s work.

With link for those with less accommodating interfaces on their spiney-go-rounds (or those who were dubious and needed to see the math for themselves).

edit: …and the math for those who are not quite curious enough to go look, but might absorb it if it is right in from of them…now that I have a keyboard.

RCF = 1.12 x Radius x (rpm/1000)2

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For those wondering, Carol is the name of the fuge that we’ve been doing most our spinning in.

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And cyclops plays some more head tennis with a fish

Btw thx guy for saving an excelent thread from going…

I had a basket of 25 micron felt made for lanphan China fuge with a smaller top entry hole and reinforced top side
Until the sintered stainless model is finished
(16 weeks :cry:)so far so good

It can hold a max of 15 kg of crystals
More and the layer get s to thick to function properly and fast

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Nice bag.

Hmmm… bag or rotor?!?

This style rotor is more appropriate, but if you’ve managed to build a bag that works I’d love a copy.

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what is the ideal centrifuge to spin stainless jars this size?

ideal?

that would imply I have spun them in more than one.

we had a fuge. we found “not glass” that fit.

anything with 98-100mm diameter buckets should work.

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makes sense. I just want to be able to spin more than those tiny 50ml tubes. cant get any real work done at that size

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there are multiple desktop and floor model centrifuges that take rotors similar to this

https://www.djblabcare.co.uk/djb/product/610/Accessories-A4723-4_x_600ml_Rotor_Obsolete?productstocktype=0

4x 600ml or 6 x 600ml should get you buckets in the right size.

1000ml buckets exist, but then you’ve got to use a spacer or find a different bottle.

swinging buckets are superior to fixed angle in this application, but you can generally spin the fixed angle rotors harder, so there are pro’s to both solutions.

see: Separation Anxiety (mechanical)

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