Do you mind elaborating on what you’ve discovered in these areas? These stood out to me, and I think there’s probably some really good conversation around these points
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Lol that coa of mine has made it dang near around the world now. But that wasn’t with TIBA
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Hello
With what Then ? TBA?
Greetings?
Top secret chems 
I shared with 2 other members about a year ago but until I get some time to test it at larger than sub kilo scale I don’t want to release it.
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Color?purple?golden?
This COA is the Most beautyfull thing i saw in my life!!
This is almost a Perfect conversion
Only 0.498% unknowns!!!
Im in love 
Big respect and big Greetings to all wizards
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Check your dm’s I’ll send you the full coa image with the sample pic in it.
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That’s an amazing job. Have you tried large scale?
It’s most likely just a great example of what chromatography can do, nothing more or less don’t be fooled into thinking 98% D9 can be achieved by simple cleanup methods.
There’s no chromatogram for the CoA though, so what is meant exactly by “sum of all tested Cannabinoids” isn’t really clear. It could just as well mean “of the stuff we could identify, there’s so much of each”.
So yeah that CoA doesn’t really allow to draw any conclusions about the underlying isomerization method.
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Largest batch I’ve tried was 500g
This was an inhouse hplc my homie did on one of his runs
I have a couple different sops I need to try using different solvents and reflux times
Hoping to get out to Colorado in a few weeks to run these in a lab suited for pyrophoric substances
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Tri iso is good on all alkanes
Yust make sure your reflux temp doesn t go over 72 C for triiso will start to disintegrate
For Cbd-a isomerizations use pentane
For higher temp refluxes I preffure N-hexane
For it s bp is below the disintegration temp
And yield s are 90% + D9
DRY is everything as usuall
Dry solvents
Dry hardware
Dry gasses
DRY it all
Working on lined ss saves a lot of gas use
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On a side line
Salts acidic salts with no solvent refluxes are giving hope to friendlier reagents
Especially those derived from phosforic acid
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says who? is this the same BS like with your “lewis base” Magnesium sulfate? 
Umm that actually works tho 
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which one? mgso4 he already debunked himself
Have you ran it ?
I definitely put mgso4 in my rxns that i wanna keep dry. It’s done an excellent job keeping down minors, as well as moisture. But I don’t use it as a reactant. I think it would produce d8 in a wet solution.
But I don’t think it’s acting as a Lewis base, although my chemistry knowledge is highschool + internet
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correct. Mg2+ is a Lewis acid which strongly coordinates OH- ions
i don’t need to run it to know it’s BS
the benefits of a proper education
Ok well that’s a shame
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