Are you isolating in your lab?

No I have not I still use same sop
And it go s well it really does

2 Likes

It sure makes puuuuuurdy thangs

3 Likes

Can you recycle the amine? Or if not, how do you deal with amine waste?

1 Like

Its a great sundae topping - gives it some tang

1 Like

Do what you have to do :upside_down_face:
Done for now

4 Likes

Had that thought the other day about introducing amines to the mother liquor to push out any remaining THCA. Do you see an efficiency improvement or just a decrease in cycle time for the crash?

Do you get side reactions and synthesis out of this process? Do you end up converting amine to amide?

There is a few reactions happening in the process but all are simple acid / base reactions

2 Likes

I would recomend you have a look at the film I posted at the botom of the tread to check the speed

4 Likes

It s been in this forum for quiet a while :joy:

5 Likes

The silly billies call it “deprotonation”

2 Likes

Knowing the build quality of other items I’ve sourced from waxplug, I’d be more hesitant than you seem to be to recommend dropping actual money on something from Chemtek. Especially considering the website listing for their filtration equipment doesn’t even work. I’m sure he’s got something in the works, just not confident enough to recommend anything yet, personally.

Just make one yourself. They’re not that complicated and you can build one from off the shelf parts for less than 10k, dm for a parts list to get you started in the right direction if you’re interested. Carbonation stones aren’t nearly as expensive as some would have you believe, and sintered disks are a better topology anyway.

The real question is are you baffling your isolate in your lab?
Confused Isolate is the best isolate!

9 Likes

Definitely not the hardest process to setup for, especially with inline hydrocarbon. I’m also available for build/retrofit/design on isolators and accompanied SOP’s for your target compounds. Easily retrofit setups from 1 to hundreds of kilos a shift.

1 Like

What is it ?
A crystelizer ?
Looks cool

That’s one heavy motor on a singel small flange !!
I have personally experienced the motor ripping a 2” triclamp weld ferrule from the unit

1 Like

Basically a hydrocarbon reactor / crystalization yea… I guess it could probably use a bracketed hanger to help reduce strain.

1 Like

the hemispherical bottom was a problem when we tried it, you don’t want space for stuff to crash below the area where it’s agitated/filter plate

2 Likes

:rofl::rofl::rofl:

4 Likes

Yea lots of little tweaks need to be done to the pictured machine. Lots of cool ideas too for new features maybe.

5 Likes

The lenticular to catch your isolate?

1 Like

Here’s some pics of a smaller and a larger isolator I built with just what was on hand.

Also some of the product we pushed.

8 Likes