Time lapse start to finish Sublimator run

[Beaker]

This month was a change up. No terpene horizontal run first which is a first pass distillation. So far it has been
Step One
Dewax

Dewaxing shatter

There are a bazillion ways to dewax effectively. Here is a run I just did. My process this month will utilize counter current seperation later in the refinement chain which will use hexane, methanol, and water. So this month for dewaxing I went to methanol which really goes to town on pulling out the waxes and DNA and gunk. This month the added benefit is that the compound is then already in methanol and counter current seperation of the terpenes and such can proceed without an intermediate step…

Step Two
LLE

Liquid-Liquid-Extraction

This months med run proceeds after a dewaxing process which left the compound dewaxed and disolved in Methanol. A 100 ml addition funnel used as a sep funnel was used. Starting crude concentrate before refinement and dewaxing was one ounce. I chose to start with 50 ml of hexane on the premise that about two milliliters hexane to one gram of extract would be enough to easily hold it in solution. My rule of thumb is one gram of extract equals about one milliliter of liquid. On the left is the com…

Step Three
First pass cryogenic sublimator run

Step Four
Pyrolysis

Step Five
Second pass cryogenic sublimator run (time lapse)

time lapse

Not much left.

I plan one more step which is one more cryogenic sublimator run but at 120C on the yellow portable unit. The yellow thermocouple is roughly the oil temp. The mantle setting shown in green LED and actual temp red LED. Typically the chlorophyll by this point is removed but my flow this month skipped that step to observe difference given the change up in procedure. The compound is damn fine med right now but tomorrow I will dial in some water clear. Today was a good day brothers and sisters on Earth and now I am going swimming after a few puffs.

Compound is in vacuum storage. Peace.