ReXing THCa in pentane

Great tip

1 Like

All I can say is experiment. You can take the same Batch and crash it multiple times until you get it right. Thatā€™s what I did the first times in R&D

3 Likes

I was just letting him know how far off he was not giving a specific ratio. Which is easily altered by how clean your thca is from the mother liquor. I usually will saturate at a good ratio for room temp or cooler (depending on how cold the lab and booth are) nucleation, dissolve at a warmer temp, then drop temp ,and walk away.

2 Likes

Eg: where did your jar start?

Where did you take it by putting it in the freezer?

What does the crystal size tell you about your degree of supersaturation?

If youā€™re looking for BIG, how does the level of supersaturation you achieved compare to what you were aiming for?

Oh waitā€¦you werenā€™t aiming!

Now that the target has been described, try aimingā€¦

2 Likes

I was leaving the purity of the thca out hahaha I guess were just handing out this morning lol

2 Likes

Nobody fucking readsā€¦

9 Likes

So true I donā€™t mind dropping hints in the proper context ā€œmoodā€

1 Like

not looking to achieve big boulders just some nice diamonds so i can reincorporate back into the sauce.

i took thca that i crashed out of a ethanol mix purged the ethanol off in my vacuum ovenā€¦ then dissolved the thca 4:1 into pentane. putting it in the freezer was an idea i got from someone saying doing a temp cycle where you get it really cold then bring back to room temp then close to bp then back to freezing. then back out at room temp to finish out. i beleived i was SUPER saturated and flew passed the meta zone when i took it to -45 because it sugared out to the bottom of the jarā€¦ idk if iā€™ve said this enough but i am really green when it comes to thca ā€¦ iā€™ve been ingesting it for 2 decades but just now getting the experience in isolating it. #RookieStatus

Iā€™m pretty sure I know what you didā€¦and why.

My point is, if you can explain where on the graph you were at each step, you will have a better understanding of the process.

You donā€™t have to do so in public, but that would be my recommendation

Youā€™re not wrong here, but youā€™re also not using the graph(s) to explain where you were at each step. I suggest you print out and mark the graph up.

Is your buddy any good at this trick?!?
Their advice isnā€™t spectacularā€¦

If you were a pro, I wouldnā€™t be smacking that spoon on your knuckles repeatedly.

:shushing_face:

6 Likes

Question (for anyone):

Iā€™m looking to produce large quantities of diamonds. I think I need upwards of 200kg per month, which seems like an insane quantity for jar teks (but maybe Iā€™m wrong?) in terms of pure management time.

Has anyone gone to a scale like that with diamond miners? Iā€™m contemplating 6-12 of these 1.6L miners from a place like BVV.

1 Like

200KG of raw THCa or diamonds and sauce?

1 Like

I want to end up with 200kg diamonds - the material I am starting with is about 98% THCA.

Ive seen people crash in 100L reactorsā€¦

1 Like

Across 16 vacuum oven
And 1 stirred reactor
Buchnerfunnel or filterskid
And a Bunch of Pyrex oven dishes
Would be my bet for 50 kg a week
Of diamonds

2 Likes

300L :sunglasses: but diamonds shallow is best
No agitation if you insist and pea size is good enough
2 solvent system pentane on top of water spiked glycerine
Slight agitation but with a Stratton
So no mixing of liquids occure low rpm

6 Likes

Hereā€™s another question I havenā€™t seen anyone talk much about - not too sure how to search for it either - but how do people typically handle the offgassing of Pentane and other solvents into the atmosphere from diamond mining - does anyone go crazy with C1D1 lab units or is the amount of offgas pretty negligible from smaller diamond miners and mason jars?

We have monitoring in place for air quality in our lab.

2 Likes

We also have air monitoring in place. In our (extremely well) ventilated lab, weā€™ll open up our miners/jars and have never caused the LELs to go off.

That being said, the majority of our processing takes place in a separate C1D1 booth.

4 Likes

I just recover all the pentane I use from the vessel itself

11 Likes

^^^^^^ right way to do it.

Into a vessel on a scale so you can learn the correct rate is helpful tooā€¦

:shushing_face:

12 Likes

Thats how we roll

2 Likes