I’ve tested a method and was able to separate THCA from the terpenes. But now I have these wierd looking crystals. So I attempted to further refine and recrystallize using heptane but wasn’t successful. I essentially dissolved 5 grams of the thca into a small amount of heptane, then put it in the freezer over night. I had hoped it would have recrystallized overnight but there wasn’t any solid formations, just a gel like substance. So I filtered it through a coffee filter but now I’m not sure what to do other than evaporate the heptane.
Does anyone have any experience in further refining THCA for clarity and size of diamonds?