So I’ve got some material here that refuses to stop bubbling, I’ve ramped my roto bath up to 165 and it’s been running like that for three hours and prior I’ve had about 8 hrs of it at 140-150, everything had been performed under vac.
At first I was guessing maybe residual etoh but by this point there shouldn’t be anything.
Just as in today/recently? Cause this is some stuff from a few days ago. Or just as in etoh is removed? Cause there isn’t anything being spit out by the diaphragm pump or collecting in the flask
I feel like maybe the 60rpm is what’s causing my time to be lengthened so much… perhaps. This is why I need to order domes or fab some cheap shit out of tin…
But I dunno, I’ve been wrong before and I’ll be wrong again I’m sure lol