Filter Tube for centrifuge ( THC Isolate ) (need help)

Yes, sir, I agree with you. I didn’t extract it directly into plastic. Since I didn’t have a second jar, I fit some oil into this one.

It’s not fully purged. It was extracted with butane (Open Loop), then was purged with a hot water bath for a long time**(near 48hrs keept the oil around 40-60c). After that, it was transferred to jars.Also, I extracted it about 30 days ago, so some butane should have evaporated by now.

ps**: My vacuum pump stopped working so i made to purge / keep them like this until now.

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Running stuff that hasn’t seen vac yet is my preference.

Solids will be essentially purged after centrifuge ( I decarb under vac, so no purge required).

“HTE” may or may not need to purged post separation. Depends on how much solvent was in there and which fuge it was run in/what temps it was run.

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Ty for information.
I understand these much better now while I’m doing it…

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Not your average optical bench…
But clearly in situ spectroscopy.

“Moronnabis” reports that there is evidence to suggest nanocrystalline dispersions.

And that “butane works but no theory”…

https://doi.org/10.1117/1.JBO.18.4.046009

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@cyclopath Am i going well ?



Each picture was taken after 1.5 hours of a run (2 x 45 minutes). The last picture shows what happens after nearly six hours

My fuge process is taking a little longer than I imagined. I’m running it for 45-55 minutes each round at around 3400-3600 RPM.

(*i cant go above 3500RPM , my Fuge start being little noisy and im living in an apartment…)

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I refer you again to YOC Dirty Diamond Tek - THCa isolation from Crude

Those 5x10^6 G.sec take me a couple of hrs….

I don’t understand what that means…

You’re spinning each batch 2x 45min?

Or

You’re throwing a second batch of “sugar” on top of one that has already been spun?

To what end?

They look like progress, but based on those pictures id probably recommend 15x10^6 G.sec to “overnight”.

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Hahaha, the second guess is crazy! wonder if someone try that.

I posted three pictures; each picture shows 1.5 hours of a run (2 x 45 minutes). The last picture shows what happens after nearly six hours.

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Have you seen the equation for calculating RCF?

It involves the square of the swing radius. You’ve got all your stuff at the top of the tube, where the G’s are less.

Couple or 3cm further down the tube and you’d have more joy.

Note: got it wrong here (Doh!!).

It’s RPM^2

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Ty for the hint!
cant wait to try this with bags.

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My team seems to think I’ll spin almost anything…

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fak i laugh so hard

Your team made a custom ( Dont touch ) label for u ,lol

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@YPSIOIL Hey Ser, Could you please confirm if I can use a mixture of 70% Butane and 30% Pentane to nucleate crude oil? Will the butane be helpful, or will it evaporate and its useless at all?

Pentane is all you need, put on a heat pad or oven at 90°f for a few days

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Thanks for reply🫡

Guys im waiting for my filter bags to be delivered, so I might end up wasting time and doing some crazy things.

After spinning for more than 24 hours, I decided to stop and check everything inside the strainer. Here what I got:





fuck im sooo high this post might take little long to edit…

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youre going to need to do some pentane washes and re-x’s to clean that stuff up. i played with similar quality extract to see if i could clean it up. after this stage i dissolved everything in warm pentane, crashed out as much as i could, filtered out the gross stuff, added more pentane and repeated the cycle

also you literally answer your own question here
Also my second question is which filter press bag is the best option for this method ?
5 - 15 - 25 micron

ps: ( i study alot in the forum for this method everyone is using 25 micron Bag, but i could not find an answer if 5 , or 15 micron can be a better option because you saw everyone uses 25 lol )

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How many G’s?

Take a tape measure to it…I’m guessing the radius at the bottom of your insert is at about 10cm.

ReX helps a lot if you’re looking for isolate. You can definitely spin the shit out of poop soup if you’ve got the right tooling.

Note: the “squared” is on rpm not radius.
I got it wrong upthread.

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Okay soon i get this:
https://www.merckmillipore.com/FI/en/product/n-Pentane,MDA_CHEM-107177?ReferrerURL=https%3A%2F%2Ftamadkala.com%2F

durrr

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My experience with 5 and 15 is that they are SLOWER which is expected. And I did not see a noticeable change in quality. The only time I use smaller than 25 at this point is if I’m screening for microorganisms, and then I’m using a 0.5micron.

Something else I noticed is that bags have different seams and seams have different values as well - so you should ask about that. Your 25 might be 20 micron material with 25 micron seams, for instance.

I’ve also used MUCH larger micron bags/screens (similar material to my bubble bags) and much larger filter types. And I’ve used dozens of different filter media and filter papers. They all do different things - some slow things down, some speed things up, some absorb stuff, some let the waste through and hold onto the gold.

So understanding what you are trying to achieve - how its not working for you - allows you to pick a better tool (bag, filter, media, whatever).

You want a bag in this instance that will allow the bad stuff to flow out - while keeping the dried material inside. Depending on the size of your crystals - you could go bigger here (there are screens instead of bags out there for fuges).

But from the photos it looks like there is some other stuff going on there. And everything is fine crystals (again from the photos…) even though they are sand castled together after running overnight. You’re probably getting some intense crushing going on there, which will change how things “look”.

25 micron is commercially available and easily accessible. Doesn’t mean you can’t do a DOE for your own process and see if different rates would work well for you.

I think if you were using a 10 micron with the material you have here, it would have run slower and you’d have more layering than you see in the photos.

So keeping plugging away at it. And let us know how the adventure goes! <3

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partial decarb seems to decrease crystal size (early termination?)…so old material plugs some filters faster

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