Distillate Recrystallizing

[NewLevelProcess]

Something was in your flask when you distilled that nuked your load.

[cyclopath]

not sure I follow you…

how many COA’s do you have?

you took 90% TAC, diluted to 80% TAC

let it sit, now it’s at 24% TAC?
…but you learned this by looking at the COA again?!?

@DrWHY420

I made some some distillate that was 90% total cannabinoids,

@DrWHY420

then used all of it to make flavored distillate cartridge oil, coming at 80% total cannabinoid

@DrWHY420

I looked at the test results again and noticed that it had 22% d10-THC.

@DrWHY420

There is also 2% CBN and no other cannabinoids detected.

[DrWHY420]

I have 3. Its at 80% TAC 22% d10 58% d9

[cyclopath]

@DrWHY420

I have 3.

so by

@DrWHY420

I looked at the test results again

you presumably mean you retested it/had it retested?

was the D10 called out in the first two tests?

[DrWHY420]

Yeah there was d10 in all the tests. Does d10 crystalize?

[cyclopath]

D10 fully crystallized?

Purchased some d10 and it bloomed and became a fully solid crystal in an interesting structure I haven’t seen before. Is this normal of pure d10 or is this something else? [received_786175556123276]

[DrWHY420]

Any idea what “nuked” my oil? I got some BHO from the extractor processing some new material. I winterized it in ethanol, and used a paper filter that is labeled “slow” to remove solids. I processed the winterized infused ethanol with a rotovap, decarbed, then distilled the winterized crude oil.

[TheVanillaGorilla]

I would say chances are it was running through CRC and got contaminated.
Next time try to wash it before running it through any heat process.

[cyclopath]

Not made from this (or last) seasons Nor Cal harvest is it?

We (re)learned of D10 via phoscheck.
Which is a fire retardant…

See: Delta 10 THC

@Shadownaught

The first D10 theory was based on the fact that outdoor material from Nor Cal seemed to produce high D10 levels. The theoretical explanation was that Phoschek from fire zones was to blame.

@cyclopath

@Genesis1-12

Also I left out that I worked at fusion farms LLC which was the company that first discovered Delta 10 THC.

Yeah no, that was Mechoulam et al.

Base-catalysed double-bond isomerizations of cannabinoids: structural and stereochemical aspects - Journal of the Chemical Society, Perkin Transactions 1 (RSC Publishing) first describes that synthesis…

[cancaKilla]

Some sort of plant reaction to the retardant.

Delta 10 THC: What Is It and What Can It Do?

[cyclopath]

Ignoring the giants on whom’s shoulders we are perched huh?

@cancaKilla

The fuck it was…

@cyclopath

that was Mechoulam et al.

Base-catalysed double-bond isomerizations of cannabinoids: structural and stereochemical aspects - Journal of the Chemical Society, Perkin Transactions 1 (RSC Publishing) first describes that synthesis…

@cyclopath

We (re)learned of D10 via phoscheck.

[cancaKilla]

Hell no Cyclo!!! You are my ace 1 until thee day!!! I was googling and wanted to add,lol. I’m not a slouch but I’m humbled!!! Salute Jedi!!!

[pdxcanna]

Has anyone done a standalone test with phoscheck vs sulfur?

I’ve heard conflicting opinions on whether or not phoscheck will cause it

[DrWHY420]

This is indoor. Maybe something else like Sulfur. I’m not sure what converts it.

[cyclopath]

Could be. CRC media making into your boiling flask would also be on the list.

[NewLevelProcess]

How do you clean your glassware?

[ParExtracts]

I have had this issue and converted 20L of good D9 into around 50-60% D10. The flower that was extracted had high levels of sulfur.

When you were distilling, did you have a slightly stronger odor? If so that would indicate sulfur, which happened in my run.

[ParExtracts]

Also had issues with CRC, yet this media only converted D9 into D8.

[ParExtracts]

Our solution was to add in copper when doing our winterization to remove any sulfur.

[Chemistreeclub]

Could be hydrogen peroxide sprayed on flower but difficult to know for sure , same with foliar phos . Youd know if it was sulfur, it coagulates ontop of decarboxylated crude . Basically anything on the plant reacts during decarb and distillation.