debris and frozen water droplets in recovery

[cyclopath]

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Molecular sieve beads

I bake at 300F, over night, under vacuum. I doubt that your nitrogen sweep is doing much to remove water from the beads unless you’re heating it first. it is simple enough to test. take a handful of your dry beads. add a 1/4 cup of water. if you don’t have to drop them on the floor because they get too hot to handle, then they were not dry to start with (the absorption of water is exothermic).