must sleep its nearly five am here.
talk soon.
must sleep its nearly five am here.
talk soon.
I cheated my way into not having to learn French. That was difficult, is our neighboring country, hereditary enemy and hereditary friend (hereditary brother), but there was a trick with religion in my time. Then you had to learn the Bible, but not French. Well nobody got around to English, everyone should have been able to do that … And you can see how well I can do that … namely exactly 0;) Ok, 0.5% … xD.
But I’m pretty proud of being able to read the Bible a lot less: D
The language of science cannot be put into language.
Oh sure, 5 o’clock but then it’s about time
Here it is 9 o’clock in the evening, sorry that I’m too much;)
Sleep well until the days.
OTC baby ![]()
to give others ideas of ways to do the reflux.
there is a pasters pipete in the silicon stopper as well for inert gas to be inject if I want to run
one of rogues methods ![]()
ill put up how I stir for everyone as well so they know how to do it without a hotplate stirrer when
reaction is finished.
the dish with the oil in it is made from aluminium so I can stir through it.
I used to use a cornings saucepan but with the way things are now I could not get one in time.
it was a camping kettle that I cut to size.
hence the lip on the left which was the start of the spout.
I use it to hold my thermometer so I can measure oil bath temp.
I do have a full lab set too of glass but I want to get this down with out it.
6 grams of full spectrum CBD brown isolate
200ml of IPA
2 grams of salt
7 well formed drops of Sulfuric Acid.
1,5 hours reflux
product feels like I put a felt hat on my head ![]()
warm stone much much better than the 1 hour product.
I wonder if tolerance is going to be staved off better with a full spectrum.
if so I shall be mixing the two then trying with terpenes to change the properties of the oil
to see if I can emulate the effects of changing strains of pot for tolerance removal.
1.5 hours is the spot I think.
we have some research done above by jeeric which would suggest such as well.
oil was a lot thicker.
I noticed in another thread some one mentioned people think that THC D9 with CBD looks like water
with crystal in it (fairy floss is how I would describe it). I have found this to be the case and I would
call it a shore sign of under reacted.
there is so little acid in these reactions that I am lead to wonder if there is enough
in there to crack a medium sized tri glyceride ![]()
it may be possible to just chuck a bottle straight in and then deal with extraction of reacted
product later.
I bet beeing diluted by alcohol would only help in the extraction of the result.
freeze down alcohol in the freezer over night.
filter and then dilute with water and extract.
this is the spectra from an lc of the 1.5 hour reaction.
I was given this in my messages but was asked to release it anonymously.
Thankyou to the person who gave this to me.
you will notice we have very little D8 I was told that the reading for D9 was around 56%
but something to notice other than a heap of other small peaks is that the third peak after
the D8 is as large as the reaction done for 2 hours.
I wonder if there is a step between the D9 and D8 that THC goes through dur in isomerization.
I shall leave that to dr jebril to contemplate as he is the person here that will know
the most about that I think.
I would think that we have a choice.
a majority of D9 or a mix of D9 D8 but the reaction seems not to go over 60% D9 either way.
next to try the boric acid I guess.
I may also not there is a huge difference in the high if using a full spectrum extract rather than
pure isolate.
the one worry is all of these small peaks showing side reactions.
I wonder what the acid will do to the other compounds in a full spectrum.
still this does not take away from the fact that the full spectrum seems to be a better high
and does not seem to build tolerance as quickly (it still does build tolerance though)
I should also note that the CBD levels were reported at 2%
so we have 2% CBD 2% THC delta 8 and 56% THC delta 9.
CBD and THC delta 9 both have an optical rotation measurement around 130 degrees
so I think I should get a reading of around 130 degrees when I put it through a polarimeter.
this is of course depending on the rotation that is effected and observed for the other
side reaction products.
at a guess I would say that the rotation then has a lot to do with where the double bond is
as both delta 9 and CBD have the same rotation and the double bond is in the same place.
this is a guess though not something i have dug up out of literature.
What do your comments have to do with anything in this thread?! Who and what are you responding to?! I do not appreciate generalizations being directed at me, most especially ones insinuating that I am some kind of stupid nazi fuck!
@cyclopath, @sidco, @Future… one of y’all feel like splitting these comments off? Thanks in advance. Much appreciated.
Shall we quote something that doesn’t need to be here as it’s history or can we get along & get back to science, German ancestry is a past that doesn’t have a place in today’s times especially with science afoot!
The people you refer to are not us. You are barking up the wrong tree. Please stop. You are detracting from any discussion relevant to the thread’s intent.
Then go do something else about it. Your time is not being spent well doing this here.
Of course, we know. We’re in the cannabis industry. We’re not the other side.
Wow, and you dont think you sound arrogant as fuck? How can you do that and call other people arrogant lmfao.
wow did not see that coming.
I think I would like reference an old post with a legless lizard.
you can never tell.
my grandfather was a prisoner of war for 3 years in poland in the camp next door to
auschwitz.
I hope that myself and my siblings have manged to “outgrow” the problems that this caused
my family.
still I have bedded a few germans and been friends to many.
that was yesterday man not today.
the humanitarian acts that germany does is above and beyond.
humble and empathetic is what rules the world as the more civilized people
become the more gentle they become.
if you think america is in control of this world your are as much a victim of media as some
others here.
global economics is what drives countries GDP.
so I guess in the end it comes down to if you don’t like it don’t buy it.
still if we end up in war with china things will go right back to the start again.
lets hope that all the efforts that have been made to make us all friends was
enough to stop such a thing from happening.
its better to love than hate.
it just makes for a better quality of life for your self and everyone around you.
I think we have a trolling issue on the forum. It could just be my paranoid mind at work but there’s been quite a few instances of this in the last week. They could be connected. Idk, what do you guys think?