It was 2017/2018 so things were way different and analytics were also very frustrating.
Buying solvents wasn’t as easy. Alibaba was the source for most things. I’m glad things have gotten easier and knowledge is out there with people helping eachother
I’m super ready to dump this data on the magSil in the trash and try it again …but I’m not in a lab nor near any of my equipment. I do have material still if anyone wants to play with it
I have loads of data from pesticide remediation projects.
The sad truth is that cannabis pesticide regulation is as simple as avoiding the pesticides on the list. There are probably a dozen of other effective pyrethroid pesticides that aren’t tested for in any state.
When foods (strawberries) are tested it’s not done this way. When a new peak is detected it’s quantified and checked for permitted use. You can’t just dodge regulation by buying bifenthrin 2.0 which separates slightly on the testing methods from
Bifenthrin 1.0. In cannabis that’s all good.
So It was definitely bifenthrin that’s I was able to remove using this technique, I’m getting the initial RD samples and the post remediation COAs together on my desktop Will update soon
Simplest way to “remediate” will be to crystallize the THCA out and discard the filtrate, test that the crystals are clean, and find some way to work the THCA into another batch. Working with adsorbents and chromatography will be extensive in scope and probably still never quite work. Crystallization is going to be the only single-step separation that yields anything you can use - you might be able to salvage the THCA but the terps and non-THCA cannabinoids are probably not salvageable without a lot of money/time lost.
This is from the standard MagSil PR LLE pesticide tech that everyone uses a variation of.
There is another solution that’s the wrong answer, but you could always just dilute the living crap out of it until it passes if your type of metric track systems allow for batching like that.
LOQ is not the same as “passing” although most labs set their LOD as close to the legal limit as possible while still being able to quantitate at that pass/fail threshold.
it costs more to look harder
nobody wants “it passed but we can still see it” on their product.
So you have also likely used product ABOVE LOQ as well…
Be mindful that in some states - dilution is illegal. Like in Michigan. You have to present your remediation plan, it will be denied. And if you get caught, you will get a suspended license and a big fine. This happened to someone last year, who shall not be named.
Always good to consider the regs in your location before you select a course of action. Some states don’t allow you to remediate pesticides at all and will be looking for that less than 30 day destruction log.