I have a client with a need. Recommendations welcome!
That’s BIG…
Can you clarify a bit? Largest one’s I know commercially available are 5L
What about the one that Sohxlet had?
He had that big one he was looking to sell that process two pounds at a time
Guess it’s not too crazy after-all! Wow!!!
Do you know your way around this equipment and associated methods?
Not at this scale… Best of luck though!
It wouldn’t tag him when I tried it I don’t know why
Wasnt there a guy on here who made a tri clamp soxhlet?
Not that big iirc, but with stainless you could probably just scale the whole thing up…
My 72L setup is in storage collecting dust. I’d love for it to find its way to a good home…
Hello,
This is Sindy from Shanghai Linbel Instrument Co.,Ltd.
We are manufacturer and have specialized in chiller/rotary evaporator/jacketed glass reactor equipment since 1998.
Please contact me for more information,we will introduce the most suitable equipments for you.
Sindy Zhang
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I’m sure you’d have some trouble making something like this without at least one custom length spool so the spacing isn’t off.
I would approach this by making it out of stainless triclamp parts off the shelf. You can have a 12” spool as your material column, an end cap that goes to a u bend with 1.5” as your siphon arm, then return to your boiler. Same with the boiling arm.
A 30L glass vessel sounds like a disaster waiting to happen.
Just FYI. When you do build your monster soxhlet add an external heat source to the side arm where the vapor travels up. Large soxhlet tend to reflux when pushed to high requiring more energy from the mantle, even the you can’t take a solvent past it’s boiling point the excess energy can cause products, mainly alkaloids to degrade with long extraction times, if money is not a problem one could have a short squat soxhlet with a sprinkler style head at the bottom of the reflux condenser and fix this.
We can make a big glass Soxhlet setup
I’ve got my friend looking at this post. He’ll reach out if he’s still in need. Thank you!