@Waxplug1 thats your q
@Waxplug1 /Chemtek has em. They call them sweating baskets. Still vapor reflux but the other ones you can find are for cold brew coffee and they are too long for any normal jar
Ah yeah I saw the sweating baskets on chemtek and thought they were just for triclamp.
Cold brew coffee baskets definitely seem too tall
But this is exactly what I was envisioning. Chemtek baskets with triclamp is the safer option for sure.
those silicone seals would be problematic in this application.
neither terps nor alkanes (butane, pentane, etc) are a good match with silicone.
I just setup a cold brew coffee one literally right this moment because I finally got some more pentane(the one thats like 5inches tall). im just using it with one of the big ass ball jars so theres plenty of clearance.
Why?
What are you ACTUALLY trying to achieve?
Because i associate evaporative crystallization with heat
hmmmm.
Depends on your solvent
heat is also a fluid term depending on solvent of choice.
Pyrex tech with pentane. 4 days, no seeds
Very nice. Welcome to the future @AlbinoLobstah814!
Very nice.
extracted with pentane or that was your secondary solvent?
if secondary, what’re you extracting with, just tane?
Dang those look nice! Just let all the pentane evaporate in the C1D1?
Thanks man!
Secondary, Extracted with just butane.
Yessir
cold fresh frozen run? or dried biomass?
nice work
Fresh frozen
Not sure if this has been answered but I’m looking for a
When recrystallizing using a super saturated solution in a closed vessel could someone share their timing system for cooling to achieve larger crystals? I keep getting sugar from sugar but would like something a little chunkier.
Like for example: from super saturation temps, reduce temperature 1 degree every hour until -??C
I’d like to avoid the evaporation method, but that’s next lol
Thanks in advance
You are to super saturated dropping temp won t do much good either start at rt and stay there until you get the diamond formation
So add some solvent to slow down a bit
Remember that a transfer might be needed if to many nucleation points start to show