Hey!
Could you help me understand the effects of CBND? Is the “5x stronger than d9” just a theory, or has anyone tried it?
Thanks!
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…bump 
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Rxi-35 Sil MS Column (Fused Silica) 15m x 0.25mm x 0.25um
(VWR Catalog Number: 10058-458)
H2 Carrier on FID
140c initial temp, ramp 10 deg per minute to 180c final temp
180c ramp 33.3/min to final 280c
280c ramp 5/min to final 300c (Get ready for bake out - not so hard on the column)
300c ramp 20/in to final 340c (Column bake out - cleans the baseline)
1: p-Chloranil 1
2: p-Chloranil 2
3: Methyl Stearate (Internal Standard)
4: CBDv
5: CBT
6: d8THCv
7: d9THCv
8: CBND ***
9: CBL
10: CBC
11: CBD
12: exo-CBD? (No CRM, created during reaction)
13: exo-THC? (No CRM, created during reaction)
14: 6a10a
15: d10THC
16: d8THC
17: d9THC
18: CBE
19: CBG
20: CBN
21: DCBF (Literature)
22: CBF (Literature)
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How many ml/min H2 flow?
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Set to 23 on the gc, but I believe that is in PSI not ml/min.
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Most likely…
Detector end of column and a “jumper” in a 40ml VOC vial, with a calibrated “catch tube”.
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I will give that a go here when I get it hooked back up to the H2 tank. Have everything needed.
As a general calculation using the GPT it came up with 7.24 ml/min at 23psi and my column specs.
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Any interest in the hydrogenated H2-CBND?
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