I just saw the pic and thought it might help a little.
Boil off the solvent until itās reduced enough to see oily solution on the walls of the jar when you move it around. With too much solution youāll get very little/no crystallization
That is possible I had two lids buckle, so finally I put one on top of the other and put two lids at the same time and that stop it from buckling
Thanks you man, I realized that was my problem last night, I had WAY too much in there. I also think I should have done a larger run
Yeah your glass would be in a billion peaces WAY before you got anywhere in the ball park of 250psi.
sorry for the misinformation donāt use a prv on a jar lid
A prv is fine but one that pops at like 5-10psi Iād imagine
Like @WolfeXtracts said the glass would def bust before it hit 250psi. But before the glass bust the plate lid will bend and buckle sliding itās way past the ring lid. Ive shot em off before bc the pressure. walk away and hear boof! A prv set to the right low psi would have prevented any this
But @GroovyOctopusLabs prv fine just not that one,
Your pops the relief at 250psi which is a ton. This one pops at 10psi. See the difference?
Might be a lil betterā¦I couldnāt find a 5 psiā¦ I know oss use to sell an adjustable. But it was pricey