You have a KCA COA for me?
What if itās isomerized with KOH instead of a strong acid like p-TSA?
KOH is a base though? Would act the same as an acid if were to be used in this process? They say itās strongly alkaline because it comes from the ashes of fires apparently, so would that cause it to act like an acid in an isomerization attempt?
This seems like a great idea, and thanks for throwing it up because I learned some good shit!
Iām foggy on the science, but a buddy was talking about how CBD, methanol and KOH changes the chirality of isomerization to create D10 instead of D8 with a strong acid.
Oh WITH the acid! I read it as IN LIEU ofā¦ It is interesting how the base donates the OH (I believe it is) so that might be why itās passing over 8 and going to D10. Itās all super interesting, but itāll be knowledge I donāt think Iāll every use. Still trying to decide on the Industry, or construction
Iām far and away anything from knowledgeable on the subject.
My understanding from the literature is getting the cannabinoids into a super base and running cold, they ran at 0c. My guess is that reduces the undesired byproducts.
Wonder what KOH in the boiling flask during distillation would do
Shiii mane Iāll take all ya D-NuTZ. Whats that cannabinoid %
Last post is koh in methanol
I cant confirm thatās d10 though as Alex was mis identifying d10 and 6a10a till recently
Isomerization isnāt chirality
Acids donate protons, bases pull them
When we shift the double bond on d9, a hydrogen attaches which causes the d9 double bond to shift to the more stable d8 double bond position and another hydrogen pops off
This is why you can use a tiny bit of acid and make d8, the reaction will keep going till its stopped or an equilibrium is reached
D10 is made by pulling hydrogens
Specifically ones off the top carbon sticking out
This causes a chiral center and a chain reaction happens that shifts the double bond the opposite way
This same process on cbd makes d8 cbd (NOT cbd quinone)
This is a very basic breakdown
Ayyyyyy
Sorry, couldnāt help it
Like I said- second hand conversation on the science, not my own. Thanks for the explanation.
We mis identified a few samples for sure. But weāve pretty much chased the source of those errors and what causes the mystery peaks in manufacturing
I donāt think you had any samples that turned out to not be d10 but maybe. Iāll look again
I found the round we misidentified and we do know now itās either not d10 or itās a stereoisomer. Iāll send you updates soon. 90% of our d10 tested has been accurate but these ones slipped by for sure
I actually found the last sulphur reaction I did, im going to send to KCA and you for testing
I dont think your patent is accurate tbh youāre not gonna make 6a10a without acid in there
This is SAD.
Our customers have been asking for it. There are people who say they have it but I just donāt trust it. If anyone DOES REALLY have it, would love to get a sample to do test and then buyā¦ that as well as any other cool variations
Iāll send a d10 sample yāallās way. Your sales rep told me yāall got hella people asking you for suppliers. Woulda sent stuff in a while back if I knew that
Spare an extra sample? Iāll test it for free if I can post the results on here.
Me as well.
Would pay for samples. Please pm me