Here was the SOP described above
- Start with 100mL of DI water
- Add 22mL of Glycerol - wait till mixed
- Add 33mL of Grotek - mix for 5 mins
- Add 13mL of sulfuric acid (99%) to lower the pH
- Add 25g of Carnitine (pre dissolved 25g in 50ml of hot DI water, let cool)
- I have redone this as it was perfectly clear but then gelled up a week in.
- I have now added 40g of Carnitine HCL in 50ml of DI water and put it in a ice bath (<30 degrees, around 15-20 C I got it down to)
- I also put the grotek and glycerol on a ice bath so when adding the sulfuric acid it keep it cool, i noticed this may have reduced the tendency to polymerize (may have just been coincidence)
- So far about 5 days in a all 4 samples clear and stable.
Variables are doubling the glycerol, all 40g carnitine, 15ml and 33ml grotek variables.
Thanks for calculating the Si, i have not done this yet until i get a stable formula then ill go and calculate it. What is your math to get 1.5% and if using 99% Sulfuric acid how much S?
how many ml would i need to add of 17% Si Growtek per 100ml to be equivalent to your 4-5% Si formula mentioned previously ?
Thanks Daniel.