Let’s put all that “it’s dangerous” aside. We all here must understand the important of safety, but we chat about dangerous reagent.
TIBAL SOP in a way… In my head looks something like:
Dry CBD + HEPTANE with CaCl2,
Dry all glass vessels with hair-dryer and vacuum > then refill 3-5x times with argon
(important to leave small amount of vacuume)
Do syringe sparge with argon, refill 3-5x times.
Take some ML of TIBAL, (i guess it should be not that big of an ammount %)
squirt it thru rubber stopper.
Everything cold like -5c,
react for some time (idk how long)
then neutralize - as some dude said regular water should\may neutralize
(BUT TIBAL REACTS WITH WATER, SO I’ll NEEDS TO FURTHER STUDY)