HHC coming out runny

Running hydrogenation with a flow cell and D8 looks to be turning into HHC by the hplc but instead of being stable it is very runny like a CBD anybody seen this?

Looks like you are making more than normal of the other isomers.

And making an additional isomer, I would suggest running a longer method. Ours is 20 minutes.

2 Likes

So change my method time to take 20 minutes on the hplc?

You will just get better seperation, I can get my SOP if you want to look at it.

3 Likes

That would be great thank you

1 Like