Do large scale Ethanol Extractors use copper condensers or just stainless steel?

Yea, copper’s wide but limited reactivity is why it’s used spirit distillation, many conjures thats arent sulfer based are known to be affected by copper at least to a small degree. I just figured that very few cannabinoids will be volatile enough to make it over and almost all the terpenes in cannabis are found is another plant that has been distilled with copper condensers.

Any acidity will corrode copper, acid vapors can Co distill with etoh. Terpines on their own have no ph, due to non polar nature. When emulsifyed with water, or traces of water in etoh it can modify the ph. Try to test the pH of a hydrosol vs the separated oil. It proves the theory. Before you do the build get some copper and immerse it into a solution that will simulate operating. Get some copper test strips meant for aquarium use to test. Share the findings with us.

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i dont use water so its not really hydrosol right? the only acid they would be exposed to is the ethanolic carbonic acid but that should be almost entirely dissipated by this point, i wouldnt be able to pull a vacuum if there was any co2 left in solution, but i will try measuring the ph next time with universal strips

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Exactly!

So what if I have a still for reclaiming ethanol that’s all stainless steel except for the condensing coils those are copper. My builder is trying to say the stil would be 20x slower with stainless coils. Could I get some help on the subject?

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your still builder does understand the thermal transfer properties of those two metals.

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having decided that you’d prefer stainless, the trick is then to change some of the other variables in the equation. eg the ΔT , heat exchanger surface area, or flow rate.

@TheGratefulPhil was kind enough to work some of that math

edit: and thanks for bringing this up. I was aware that copper was more efficient, but was unaware of the magnitude of the difference. check the tiny condensers on the first still I built.

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Do I really have to go with stainless just on the condensing coils or can I have the condensing coils copper and everything else Stainless and still be fine?

This unit will be used for distilling ethanol out of the oil It is only a reclaim still so technically the cannabinoids in the oil which is left in the still will never pass through the Copper except for Turpines

@Champone I think cyclopath summed it up great here.

The problem isn’t the cannabinoids touching the copper, but rather what the compounds that will distill off with the etoh from the concentrate will do to the copper, possibly contaminating your ethanol and subsequently contaminating your extract that you re-use that ethanol for. I have had the misfortune of ending up with blue etoh when running a mash for my own personal vodka when I simply added baking soda to the wash in an attempt to achieve a more neutral spirit. Neither the baking soda nor the fermented wash touched the copper, but there was a reaction between the yeast nutrient I used and the baking soda which formed compounds that created copper salts, which then ended up in my ethanol. Copper salts being as toxic as they are, I decided to just scrap the ethanol and do a laborious break-down and cleaning of my still rather than try to clean up poisoned product. I have had the same blue ethanol problem when I try running too far into the tails, which probably means it is something with a higher boiling point than ethanol that co-distills that is pretty rough on copper. I wonder if that’s also what was causing the blue in cyclopath’s experience?

You can probably get away with using a copper condenser if you just distill off enough ethanol to move the product into a rotovap for finishing. Cyclopath stated that he didn’t have any issues with the color of his ethanol until he tried squeezing out the last of it from the extract. Hell, I use a copper reflux tower to re-proof my reclaim and I have had zero issues. But if I was going to invest the money into it myself, I’d rather just do it right the first time instead of having more expensive issues down the line.

I usually still it down to the last 10% then finish off in a roto. So I would be ok with copper?

I agree with doing it right the first time. My entire still is stainless except for the coil inside

depends what you mean by “coil inside”.
you using something like this?

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We run Ethanol only and use stainless steel for everything.

It’s a bobkabob Condenser that’s the only part that is copper all the rest is stainless

Do you run your still under vacuum

hmmm…wonder what a bobkabob is…

https://homedistiller.org/forum/viewtopic.php?f=17&t=27072

first link I clicked on. and it’s stainless!

Too many :honeybee:s in my spelling I was driving ha. Then why’s my damn builder saying I have to use copper lol? I wonder if it’s because I’ll be under vacuum therefore needing a much lower temp to cool

Do you think just bring copper on that part is a no go ? Or it could work only distilling down to the last 10%?

How are you planning to run a boka under vacuum? My column is a boka and I’d love to be able to run it under vacuum, but being LM I figured it wouldn’t be possible to have any takeoff while running, which would make it inoperable.

You have a catch can.

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