Hallo. I have some dark oili dmt and want to know if is possible to purifying on chromatography and how can I do. thanks
Just re-crystallize it… you can xtal to 98% pretty easy.
Cold crash is king
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Is a residual of many cold crash Notting come out in heptane I need to separate
So you already cold crashed all the dmt out and you want to convert the dark residual to dmt also?
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Yes. the dark residual is oil from the plant + DMT cristalizzed
@DiNKLB3RG @StoneD
@TheLastHashbender
So @Wisechemst is a friend of mine stuck with these last residuals
But as you can see there is something left
How would you recomend to clean this up ?
Which solvent or solvent mixes
Chroma?
All help is wanted
Thx
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Does dmt dissolve in acetonenitril ?
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Looks like he did STB on a fatty batch? Go the long way around to skip chroma tbh. Perform normal tritration and LLE again to separate out fats. Then basify and wash. Condense crash recover.
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Centrifuge it ?
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Haven’t tried this but I can test it
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just do a regular A/B and this wouldn’t have happened in the first place. synthesizing this shit from scratch is easier and cheaper than chromatography of even just a few grams
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Yeah well you know all the natural plant based stufff people want
But yeah 5-meo-dmt from melatonin was not to hard
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Maybe dissolve in acetone/IPA and make the oxalate or fumarate? And then freebase it + recrystallize from there. It’s a common trick for purifying tryptamines maybe he’s already tried it
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Is a residual of many extraction… I tried recrist and a/b ex on this but no good result. I didn’t try fumarate because I think is too much oil and fat inside and this makes me think chromatography .
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So this is basically gunk mixed with DMT N-Oxide. There’s no way this is going to purify, it’s time to throw it away.
To make oxalate in the same way of fumarate? @oscar
I’ve never done it but yeah oxalate is used too. If you’re dealing with a huge excess of oils and fats maybe it would be a good idea to try dissolving in an alcohol and “winterizing” like we do in cannabis!
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