Consulting needed - Remove THC from crude with chromatography

I’ll provide an updated next week

@Frankie did you ever try it? I am having the same problems

Not yet! I, did however get myself a ph-meter. slowly going the right direction…

One thing that is worth noting. My team took ~300g discolored, post-chromo distillate and we re-distiled it in the SPD. This produced a beautiful clear and light golden oil…

@JeRemediation. Send me a direct message. I’ll keep you up to date with what i have planned. I bet we could figure a few things out between the two of us.

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Does anyone have any input with running the interchim or any other chromo equipment with only using ethanol?

I know 2 labs who purchased this equipment one who spent $1.8M and after 45 days… Still calibrating and the yields are not good. Make sure to do your research

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I have used 200proof Ethanol as a mobile phase. The compounds eluted to close together to separate efficiently. I have better results with a gradient of ETH & H2O. Ive also had success with 180 proof isocratic runs.

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Was this using forward phase or reverse phase?

forgot to tag you so you would get notified @Chrondor

im new here.
i love this topic

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What was your method?

Hello, we have this , you can have a look LC-310.pdf (101.2 KB)

Do you like it?