Cheap budget tek for processing small amounts?

what is this this you speak of? :slight_smile:
was there supposed to be a link?

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https://m.ebay.com/itm/1000ml-24-40-Distillation-Apparatus-Vacuum-Distill-Kit-Vigreux-Column-With-Arm/231091970061

Sorry

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That will work, you will want a plain jane claisin adapter instead if the vig. It will take less heat, you will need a mantle with mag stir.

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Thanks for the help buddy so the vig column takes more heat to get the etoh to evap out of the mixture? I already have a heat plate mag stirrer. Would this suffice and does the mag stir go into the evap flask or into the heating bath that the flask sits in?

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If you have a hotplate / stirrer you will need to make either a sand or an oil bath. The vig column helps with fractional distillation, it is unnecessary for a simple distillation intended to strip solvents. Refinement of solvent is a different matter requieing a different approach, where the vig column would be more suited.

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So for my own setup I would want a claisin for simple distillation for lower temps on the oil then a fractional tower to clean up the etoh for reuse later.

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Yep, pretty much.

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I found some American made glass pieces on ebay for cheap I think Iā€™ll piece together everything myself. Found some 2L pyrex flasks, an aldrich jacketed 370mm coil condenser and Iā€™ll look for a 24/40 cleisen and vacuum adapter. Will I need a liebig to run with the cleisin adapter?

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Is this the setup I should go for with the claisen adapter? Wouldnā€™t I still need a condenser of some sort with the claisen adapter like a tee off the arm of the claisen and still use the liebig ro condense the etoh vapor?

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If you doing a simple distillation I would advise you to get the liebig instead of the graham. Coil condenser are used vertically, the liebig can be used for either reflux or distillation in a horizontal or vertical application.

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You wonā€™t need the bubble tube, you have magnetic stirring. I would simply add a pressure equalized addition funnel above the flask to add more etoh so you can add while running.


steamdistillation

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I am not producing distillate if that is what youā€™re asking. Iā€™m only interested in pulling the etoh from my oil at the lowest temps possible, then Iā€™ll want to refine my etoh back into the 90ā€™s percent purity.

I was thinking the claisin and liebig for simple distillation first (since it takes less heat), then the jacketed coil for reflux of the etoh after.

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Oh well darn I thought that was a vacuum port to pull a vacuum on the system but now I see thatā€™s a bubbler lol

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Both of the setups above are connected to a vacuum source.

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Were on the same page of solvent stripping here, I havenā€™t even begun to talk about cannabinoid distillation! You will want to preform a simple distillation under vaccum to first remove the etoh. If you want to refine a solvent though distillation you would add the fractional column, vaccum at this stage is unnecessary.images%20(3)

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Thanks for all the help man its greatly appreciated. Are there any products out there that work like a water aspirator but reuse the discharge water to circulate through the condenser?

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I donā€™t see a reason you couldnā€™t just place a fountain pump in your sink that is connected to your condenser.
https://www.amazon.com/Jebao-PP-377-Submersible-Fountain-Water/dp/B00887WA14/ref=asc_df_B00887WA14/?tag=hyprod-20&linkCode=df0&hvadid=222941228148&hvpos=1o3&hvnetw=g&hvrand=666373768416300929&hvpone=&hvptwo=&hvqmt=&hvdev=m&hvdvcmdl=&hvlocint=&hvlocphy=9031863&hvtargid=pla-390920418376&psc=1

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You could also go this route.
https://rover.ebay.com/rover/0/0/0?mpre=https%3A%2F%2Fwww.ebay.com%2Fulk%2Fitm%2F263751556400

https://rover.ebay.com/rover/0/0/0?mpre=https%3A%2F%2Fwww.ebay.com%2Fulk%2Fitm%2F261958046841

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Sox thanks for the heads up. Is 55 degree well water cool enough for the condenser?

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55f? Should be fine, if you arenā€™t getting good efficiency you may want a longer condenser.

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