Simply @Dr_Jebril? Have you noticed the price on amber glass flasks sir? Especially at scale. Super cost prohibitive imo but maybe not for your situation.
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What pressures are you typically using @Roguelab ?
On normal solvent/ catalyst reactions 15 psi if the intention is to run the reaction at atmospheric boiling point of solvent
When the intention is to run a solvent at a bp thatâs way higher than it s atmospheric bp then I adjust pressure needed
Butane at 45 C around 75 psi
Pentane at 90 C. 150 psi
Methanol at 90 C 90 psi
I have adjustable prv s in these ranges that are lined to outside for yust in case
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Did you know the boiling point is directly related to pressure by way of vapour pressure? the more you know
Yes I do it s my intention to suppres the boiling point so there is no need for a condensor
And no need for a constant Argon backfill
And the option of getting rxn gooing in solvents where atmospheric bp is to low
Phosforic acid on methanol or acetone
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you ran phosphoric acid in acetone?
Where have u been!?
away, not doing obviously dumb stuff like our master chemist challenger @Roguelab
acetone + acidâŚevery chemistry novice knows this is a dumb, dumb, dumb idea. did i say dumb
What it do?
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Who did your custom fabrication?
Please elaborate as to why, cause a lot of people are using this combo to make D8 and selling it
@MagisterChemist just posted it
Makes bad things.
Probably need chromatography + distillation to separate.
If not youâre likely poisoning people.
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