My first try in converting CBDP to THCP

I think I managed to find a source of AlCL3.
How long would you do the reaction for? 15 minutes like the paper sais, or?
Quenching - ice, ice,ice? Exotherm?
I will be renting a lab - and responsible waste disposal is included in the price :slight_smile:

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I also believe there is a difference between doing experiments in 100ml beakers with magnetic stirring and a rector. I believe my results in DCM at RT (which are very good) would not be reproducible in a reactor. The volume to magnet ratio is very low, so it is receiving a hell load more of kinetic energy.
I dont think such agitation would be possible in a reactor.

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Listen making it is easy
Keeping it is the art
It s tedious and reagent intensive
Trust me you are better of buying the answers
Either @Zzzeko23 or @EagleChem
I would recomend
There are far better route s with non pyrophoric reagents that are in the papers you can ask @RockSteady
For those

Have messaged them,

AlCl3 I haven’t really considered, although the paper I read looks promising
I want to see the maximum I can get out of pTSA first.
Chemistry is an expensive hobby I must say, but Its a lot of fun :slight_smile:

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Magnesium?
Zinc?

Butoxide potasium or potasium amylate

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