That’s a decarb. I do it the same way. 5l rotovap, pour into 2l spd bf. Purge and decarb at 140c until a nice smooth lake of crude. Attach spd glass and start running.
I pull 75% of 1st pass 93%+ distillate from my crude.
That’s a decarb. I do it the same way. 5l rotovap, pour into 2l spd bf. Purge and decarb at 140c until a nice smooth lake of crude. Attach spd glass and start running.
I pull 75% of 1st pass 93%+ distillate from my crude.