good luck with that. you’re mostly starting with junk. you can absolutely get something you can put in a cart, but getting anything that isn’t quite dark is gonna be tough.
interesting… so if i do something like soak the material in heptane then let gunk fall to bottom and filter off from top it i could be getting somewhere?
i dont have one but i have the budget to buy one if its possible around 500$? i dont need to do huge amounts but i guess i will process somewhere around 5kg a week or more in the future… for now not that much but soon my budget will increase alot if it works out. first times not so much…
so how can you be complitely sure its free of methanol? you let it run in that rotovap for a while? i will send to lab first if thats the case. and how much methanol would be left?
anything else you do to filter when you first extracted into the heptane? before it went to methanol and thanks alot for help i realise it will take some time but i really want to achieve this
Yes a crc filter with your heptane will make an excellent product. I’d use something from gochemtek.com . Then use alumina when u filter the methanol
But you might as well only filter the final heptane solution because it is dewaxed and your scrubbing will be more effective against a lipid free solution
Heptane does not mix with water and if your trying to dry heptane epsom salts are not something I would use, freeze the water & forget the bath salts lol