Good luck, @J12 is fairly tight lipped
I mean, they are and they arenāt.
I think they have a pretty standard approach in which theyāve shared already.
I think theyāve simply perfected their approach. Itās likely very much by feel and knowledge of input material.
Iām sure thereās a few secrets/qualitative analysis they do along the way theyāre not sharing. But I think the amount shared so far is basically saying ādo the work your damn self if you wanna be an expertā
I honestly just started experimenting until i figured out what works best in the easiest possible way. I feel people tend to over complicate the extraction process. I do a few things that go against most peopleās standard extraction procedures.
Iām down to give assistance, but have spent a lot of time figuring things out on my own. The tek iāve figured out is valuable so i donāt just hand it out for free. All of the info to do this is on here you just need to figure out what works best for you
Iām not hating brother, youāre the king of diamonds around these parts. But you are very tight lipped, which all of us can and do respect.
im guessing no then.
so what concentration of HCL will work best for this ?
Ok, so I when I ph the water back down with the hcl red oil drops out and sinks to the bottom of the now ph 5 water, what is happening?
Youāre forcing the cannabinoids and other things out of solution. Just keep following the course.
Ok, so I followed to completion, I did adjust the recipe for a smaller quantity, based on the ratios given. I used half the amount of starting extract because Iām starting with THCa thatās been pressed in a 25 micron rosin bag from crumbled or sugared BHO, which yielded a hair under 50% of the total amount pressed. Anyway, it came back nice, only there seems to be more oil in the water that the hexane wouldnāt reclaim, and out of concern I heard itās wise to redissolve in ethanol and rotovap off a few times to ensure you purge the hexane, however first run with the ethanol I think it got to hot and now it looks like a pinkish purple still very very clear, I took it off the heat as soon as I saw the color change, wondering what caused the color change?, Iām sure itās at least partially decarbed
I donāt do much with high heat processing, but based on what Iāve read it sounds like youāve encountered a ph imbalance, or youāve oxidized or thermally degraded some of your thc.
Will this process extract the cannabinoids regardless of decarb ?
Iām not sure I understand your question. This process is not for extracting from material, but for purifying an initial extraction.
Simple question, THCA decarboxylates for many different reasons (heat, time, exposure to light) becoming THC, does this process extract both or only THCA?
I make this and when i evaporate the pentane wash that have the non thca, smells realy goodā¦ they have any degradation? Maybe can be purify for future uses ā¦Make crystals and then add the terp refinedā¦
thca crystallizes. thc does not.
the patent method specifically crystallizes thca.
if the cannabinoids are not acidic, then manipulating the pH to modulate solubility isnāt going to work.
I make this and when i evaporate the pentane wash that have the non thca, smells realy goodā¦ they have any degradation? Maybe can be purify for future uses ā¦Make crystals and then add the terp refinedā¦
certainly worth trying. although that strategy will get you some of the terpenes. others will be water soluble and lost.
I will try to Extract with diethyl ether the terpens from water at 1 Celcius adding some salt to the water. Maybe some terp can recuperateā¦ or slow freez the water can push the terps outā¦ positiv pressure maybe helpā¦