Someone help me with an LLE please

Hash and Stuff Pre/Post-Processing
1

550gCrude was decarbing in a mineral oil bath and blew over the top and tipped over.

I need to figure out how to fix it, clearly will now be put in the distillate bin, but I was hoping maybe a methanol LLE would pull my cannabinoids.

Any tips?

2

Winterize it, more then likely you can get it to precipitate like that.

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3

So dilute with methanol or ethanol and put it in dry ice over night?

4

Yes then filter through some sort of media

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5

A quick Google search says it freezes at -4, you can probably use a regular freezer

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6

Celite 545 fine? I ordered some aluminum oxide cause I was planning on trying some methanol winterization and I saw most folks were using that but i have celite on hand

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7

Celite is what I use

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8

I’ll post update when I have one. Thanks man.

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9

You may be able to separate it with direct distillation, depending on mineral oil boiling point.

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10

I’ll be distilling it no matter what

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11

https://www.labdepotinc.com/p-59940-pyrex-round-media-storage-bottles.php
https://www.amazon.com/BriskHeat-1000-1-Silicone-Griffin-4-2-4-46/dp/B00UV2FU20/

so it won’t happen again

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12

I like your style!

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13

Did you get the mineral oil out with dry ice and methanol?

14

just had to winterize and filter, used ethanol

15

i had no idea i was actually just making homemade viscosity blend. who would have thunk it.

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16

At only a fraction of the cost!

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