I was talking to an old process chemist I know today. He’s always full of bizarre inventive solutions for things. I mentioned the struggles people have continually reproofing their ethanol, or using molecular sieves to dry it. He then told me that plain old cement can serve as a strong water absorbent and will get ethanol to 200 proof, as well as forming a paste that’s easy to remove. Anyone heard of this before? Definitely a lot cheaper than molecular sieves ($10 for 100 lbs retail). It sounded goofy when I heard it but he claimed to have done it in the past.
The constituents of portland cement are silica, alumina, calcium sulphate and oxide, all of which are excellent drying agents.
So I just wanted to put this advice out there and hear what people think.
Maybe worth an experiment if one could find a food grade cement ? I would worry about pulling contaminants that are lost likely in the raw milled constituents. I guess all you really smart heads with access to analytical equip could give it a look post reproofing?? Random guy 2 cents
EDIT: Good thought on the food-grade comment. I doubt there’s food grade concrete (considering it’s use), but perhaps the absorbent constituents? There must be a type of packing that would remove water from ethanol?
Anyone know of food grade dessicants that could be used for this purpose? That wouldn’t dissolve in ethanol?
I don’t think there’s much potential for these to dissolve in ethanol really. And if they did, you’d just need to mix them in pre-recovery and they’d distill out. As far as harsh reactions, it’s quite alkaline, but that shouldn’t have much impact on 200 proof (as opposed to 190)
This, there’s a chart somewhere on which salts to use for drying different solvents. Sieves work well for butane but are expensive and ill suited for ethanol.
Pretty standard A/b alkaloid extraction- the cement is alkali - they’d do well to soak the leaf in an acid solution first though and then swing it down helps to pull more alks…
Just finished the vid they do not explain this very well- the sulfuric acid is not added “to prevent a chemical reaction” it’s literally what causes it, swings ph down to create the salt forms of the alkaloids-
What are the desired specifications for ethanol purifying seives? What about isopropanol? And how do you use your ethanol proofing hydrometer to measure iso?