I’m attempting my first second pass I might distillation machine. I have about a hundred eighty grams of first pass distillate and I’m using a 500ml short path. I was running the biggest load I’ve ever done and I had to do two first pass batches, well I my second batch I didn’t clean out the boiling flask cuz I assumed THC he would be in there. Instantly I saw my reflux with a darker tone right after the first couple minutes of my run. I got a couple of shades darker distillate on my second run then I did my first.
My question is what can I expect in yield and is 180 g enough to run in 500 mL without too much loss.
Is the gracian something to worry about, ipull about 400 Mike rounds first pass.
Wood a lle wash be a better option? I’ve read much on that but have no experience on it.
The after taste/smell of this distilate is why I’m even wanting to so this. I’ve always have it but it puts much of a cough and rubbery taste to it.