I thought most used oxone? Or so Ive heard
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If you want want to help protect peopleās access to 7OH then sign the petition at the link below and consider writing a testimonial or pitching in a few bucks:
https://www.change.org/p/urgent-stop-a-national-7-oh-ban-protect-chronic-pain-patients
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Pretty sure thatās what everyone is using yes.
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Bengal rose supposedly. with citric quench.
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Bengal rose route involves a photoreactor. You think thatās practical at scale? @Etohthekid
I have seen pretty large scale UV reactors. I think was about a 400L closed system.. also I do remember KOK posting pics of oxone pallets back in 2019 or around that time. Iām guessing thatās the most common route but thereās usually a few ways to promote oxidation.
Right now Iām more curious how this synth THCa is being produced.
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Hey you still around boss? Iām interested in wholesale if your still in business.
Sent you a pm
Thatās pretty cool you developed a method that can break the 50% molecular yield thatās common with most of the known oxidation techniques. I will DM you some ideas for product cleanup that might improve the purity. I only came across one other method in a deep search of the literature that reported high yields, but I never tried it because the reagent involved seemed too expensive and too risky to handle in scale up.
Good work!
I know what youāre talking about and unfortunately the yields from the reaction in that thesis were totally overexaggerated . Either the 97% yield was fabricated or their testing method was flawed and didnāt detect the byproducts that were also created during the reaction. They only determined their yields by firing samples into analytical instruments, never by actually recovering the mass of 7OH from a reaction.
Over a year ago I paid a woman to fly from Indonesia to Malaysia to meet the author and get the full paper since the research library holding it wouldnāt share it with anyone that wasnāt a student at that university. I figured there must be something in the full document that would fix my terrible yields. What I learned after receiving the full thesis was that the reaction has to be ridiculously dilute (terrible for scale up) in order to perform optimally and even then the yields were no better than other methods.
The challenge with oxidizing mitragynine is that there are many other locations on the molecule that are prone to react with oxidizing conditions besides the 7-position. Finding something that is actually selective is challenging. It took me a long time with a lot of disappointing results before I finally figured something out.
Woah, thatās wild you got the copy of that thesis. I was thinking of just trying to track down the author and email her to request a copy.
Clays are greatā¦
Jokes aside, though: I remember listening to discussions you had about the azulene paper back when you were showing that work on Instagram. Very impressive stuff! Iām actually pretty certain that many of my favorite batches of 7oh came from your lab through to online retailers!
Itās wonderful to see you still continuing to do interesting and incredible things! Your azulene experience was fairly formative in making sure I was paying attention to a lot more and taking more notes in natural product chemistry work I went on to do since then. Thanks for sharing as much knowledge as you have over the years!
Edit: as a note, was N-protection with an EWG that can restore the amine double bound when it leaves just terrible? I always hated the idea of the hypervalent iodide route because singlets fuck up all sorts of things.
Edit2: exhaustion may have meant the above edit isnāt actually saying what I was trying to ask
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Hey there, I work for Bliss Blossom Farms, Weāre looking for a new bulk 7-OH extract powder supplier. Could You please message Me?
Interested. Please email me at jwobigong@gmail.com
Hi @JollyRoger710 . I am interested in your supplies, can you ahot me an email @ Sj@synergj.com
Im interested
Hey, I am in the market for this and would love to talk to you. Whatās the ticket on it and is it still available?